2014 : Synthesis of ZrO2 nanoparticles by hydrothermal treatment

Prof.Dr.Ir. Sugeng Winardi M.Eng
Dr. Tantular Nurtono ST., M.Eng.
Dr.Eng. Siti Machmudah , ST.,M.Eng.
Dr.Eng Widiyastuti ST., MT.


Abstract

Zirconium oxide (zirconia, ) is the most common material used for electrolyte of solid oxide fuel cells (SOFCs). Zirconia has attracted attention for applications in optical coatings, buffer layers for growing superconductors, thermal-shield, corrosion resistant coatings, ionic conductors, and oxygen sensors, and for potential applications including transparent optical devices and electrochemical capacitor electrodes, fuel cells, catalysts, and advanced ceramics. In this work, zirconia particles were synthesized from precursor with hydrothermal treatment in a batch reactor. Hydrothermal treatment may allow obtaining nanoparticles and sintered materials with controlled chemical and structural characteristics. Hydrothermal treatment was carried out at temperatures of 150 – 200°C with precursor concentration of 0.1 – 0.5 M. Zirconia particles obtained from this treatment were analyzed by using SEM, PSD and XRD …